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Article
Publication date: 8 November 2022

Nehem Tudu, Mayuri Baruah and Shashi Bhushan Prasad

Prior to manufacturing, designing plays a vital role in the selection of materials and other design parameters. Therefore, during the deposition of materials, substrate materials…

Abstract

Purpose

Prior to manufacturing, designing plays a vital role in the selection of materials and other design parameters. Therefore, during the deposition of materials, substrate materials provide support and affect the microstructure of the deposits, which may not be desirable in the manufactured product. Hence, the main purpose of the study is to analyse the behaviour of the microstructure at the interface of deposited material and substrate.

Design/methodology/approach

In this study, two blocks of Inconel 625 (IN625) and Stainless steel 304L (SS304L) metal powders were deposited on an SS304L substrate using laser directed energy deposition (DED) technique. Deposited blocks comprised 50% IN625 + 50% SS304L or 100% IN625. After deposition, microstructural behaviour at the interface of the deposits and substrates was analysed using different tests such as optical microscopy (OM), microhardness testing, X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS). An improvement in microstructure was proposed by performing heat treatment of the deposited sample.

Findings

Formation of martensite and precipitates at the interface of the deposit and substrate was observed. Formation of martensite and precipitates such as α, carbide and δ phases were observed in OM and SEM images. Due to the formation of these phases, interface regions showed a peak in the hardness graphs. Post-heat treatment of the samples was one of the solutions to resolve these issues.

Originality/value

This paper suggests the formation of a heat-affected zone (HAZ) at the interface of the deposit and substrate, which may negatively affect the overall utility of the deposited part. The properties of the HAZ were investigated. To suppress these detrimental effects, post-heat treatment of the deposited sample was performed, and the samples were further analysed. The post-heat-treated samples exhibited as reduction in HAZ thickness and had more uniform hardness throughout the cross-section compared with the untreated samples.

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